Through comparing several normal used ion exchange resin, the article screened an resin that deal with solution of ammonium perchlorate. It studied the impact of different test conditions on the absorption effect of the resin and determined the optimum condition witch is under the conditions of room temperature, adsorption time is 20min, value of pH is 6.68,ammonium perchlorate is absorbed D206resin , Langmuir model can better fit the process of adsorption .Kinetics study shows that while D206ion exchange resin absorbs ClO-4, the rate-determining step of ion exchange process is the particle diffusion control. Currently, there is no report about ion exchange resin adsorbing perchlorate yet, this article can provide reference for the theoretical research and practical application of ion exchange resin adsorbing perchlorate.